Novel Route To Synthesize N Doped (O- Phenylenediammine) Using Various Acids

Abstract

A material we set up polyofenirangeamine (PoPD) doped with different acids, for instance, hydrochloric damaging, sulfuric disastrous, formic horrendous, phosphoric horrendous, cold horrendous, and so on, including an oxidative polymerization procedure with potassium dichromate as an expert in oxidation. FTIR and UV visible spectroscopy were used to characterize the polymer components. In the case of PoPD H₂SO₄ and PoPD H₃PO₄, the FTIR spectra revealed a shift to bring down wave number, suggesting that the PoPD doping levels in H₂SO₄ and H₃PO₄ are the best. In UV vis spectroscopy, an efficient doping of PoPD in H₃PO₄ was observed. The thermo gravimetric research revealed three stages of degradation (TGA). In H₃PO₄ doped polymer, the second step misery associated with dopant deficit is considered as greater. The electrical conductivity benefits of PoPD H₂SO₄ and PoPD H₃PO₄ are thought to be the highest of all the acids. Poly (o- phenylenediamine) (PoPD) was successfully synthesized in acid by chemical oxidation method using potassium dichromate as an oxidant. The synthesized polymer was characterized using Raman spectroscopy, SEM, XRD and BET surface area. More unevenly dispersed particles of the Poly (o- phenylenediamine) polymer were observed from the SEM images