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2015 VOLUME 2, ISSUE 2, PAGES 1 – 15
Advanced preparative techniques for the collection of pure components from essential oils

Danilo Sciarrone1, Sebastiano Pantò1, Francesco Cacciola2, Rosaria Costa1, Paola Dugo1, 3, 4 and Luigi Mondello1 ,3, 4*

1Scienze del Farmaco e Prodotti per la Salute Department, University of Messina, Viale Annunziata, 98168 Messina, Italy
2Scienze dell’Ambiente, della Sicurezza, del Territorio, degli Alimenti e della Salute Department, University of Messina, Viale F. Stagno d’Alcontres 31, 98166 Messina, Italy
3University Campus Bio-Medico of Rome, Via Álvaro del Portillo 21, 00128 Roma, Italy
4Chromaleont s.r.l. c/o Scienze del Farmaco e Prodotti per la Salute Department, University of Messina, viale Annunziata, 98168 Messina, Italy

*Corresponding author. Email: lmondello@unime.it

FULL TEXT: NVEO 2015, Volume 2, Issue 2, Pages 1-15

Abstract

Preparative gas chromatography (prep-GC), as opposed to analytical capillary GC, is an analytical technique that allows the separation and isolation of natural products, specifically volatile pure components from complex matrices. Over the years, different approaches were used for this purpose, using both mono- and multidimensional systems coupled with different types of collection systems. In this paper, some of the most relevant results obtained in the isolation of components from essential oils by prep-GC, are reviewed. Furthermore, the main limitations of prep-GC arising from its daily use and the possible solutions for overcoming drawbacks, are discussed.

Keywords

Preparative gas chromatography (prep-GC), isolation, multidimensional preparative gas chromatography, Deans switch

References

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Eyres, G.T., Urban, S., Morrison, P.D., Dufour, J.-P., & Marriott, P.J. (2008). Method for small-molecule discovery based on microscale-preparative multidimensional gas chromatography isolation with nuclear magnetic resonance spectroscopy. Analytical Chemistry, 80, 6293-6299.

Eyres, G.T., Urban, S., Morrison, P.D., & Marriott, P.J. (2008). Application of microscale-preparative multidimensional gas chromatography with nuclear magnetic resonance spectroscopy for identification of pure methylnaphthalenes from crude oils. Journal of chromatography A, 1215 (1-2), 168-176.

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Rijks, J.P.E.M., & Rijks, J.A. (1990). Programmed cold sample introduction and multidimensional preparative capillary gas chromatography. Part I: introduction, design and operation of a new mass flow controlled multidimensional GC system. Journal of High Resolution Chromatography, 13, 261-266.

Rühle, C., Eyres, G.T., Urban, S., Dufour, J.-P., Morrison, P.D., & Marriott, P.J. (2009). Multiple component isolation in preparative multidimensional gas chromatography with characterization by mass spectrometry and nuclear magnetic resonance spectroscopy. Journal of Chromatography A, 1216, 5740-5747.

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Sciarrone, D., Pantò, S., Ragonese, C., Tranchida, P.Q., Dugo, P., & Mondello, L. (2012). Increasing the isolated quantities and purities of volatile compounds by using a triple Deans-switch multidimensional preparative gas chromatographic system with an apolar-wax-ionic liquid stationary-phase combination. Analytical Chemistry, 84, 7092-7098.

Sciarrone, D., Pantò, S., Rotondo, A., Tedone, L., Tranchida, P.Q., Dugo, P., & Mondello, L. (2013). Rapid collection and identification of a novel component from Clausena lansium Skeels leaves by means of three-dimensional preparative gas chromatography and nuclear magnetic resonance/infrared/mass spectrometric analysis. Analytica Chimica Acta, 785, 119-125.

Sciarrone, D., Pantò, S., Tranchida, P.Q., Dugo, P., & Mondello, L. (2014). Rapid isolation of high solute amounts using an online four-dimensional preparative system: normal phase-liquid chromatography coupled to methyl siloxane-ionic liquid-wax phase gas chromatography. Analytical Chemistry, 86, 4295-4301.

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Cite
Bibtex @ { nveo211765, journal = {Natural Volatiles \& Essential Oils}, issn = {}, eissn = {2148-9637}, address = {Badebio Biotechnology Ltd.}, year = {2015}, volume = {2}, pages = {1 – 15}, doi = {}, title = {Advanced preparative techniques for the collection of pure components from essential oils}, key = {cite}, author = {Sciarrone, Danilo and Pantò, Sebastiano and Cacciola, Francesco and Costa, Rosaria and Dugo, Paola and Mondello, Luigi} }
APA Sciarrone, D , Pantò, S , Cacciola, F , Costa, R , Dugo, P , Mondello, L . (2015). Advanced preparative techniques for the collection of pure components from essential oils. Natural Volatiles & Essential Oils, 2 (2), 1-15. Retrieved from http://dergipark.gov.tr/nveo/issue/19771/211765
MLA Sciarrone, D , Pantò, S , Cacciola, F , Costa, R , Dugo, P , Mondello, L . “Advanced preparative techniques for the collection of pure components from essential oils”. Natural Volatiles & Essential Oils 2 (2015): 1-15 <http://dergipark.gov.tr/nveo/issue/19771/211765>
Chicago Sciarrone, D , Pantò, S , Cacciola, F , Costa, R , Dugo, P , Mondello, L . “Advanced preparative techniques for the collection of pure components from essential oils”. Natural Volatiles & Essential Oils 2 (2015): 1-15
RIS TY – JOUR T1 – Advanced preparative techniques for the collection of pure components from essential oils AU – Danilo Sciarrone , Sebastiano Pantò , Francesco Cacciola , Rosaria Costa , Paola Dugo , Luigi Mondello Y1 – 2015 PY – 2015 N1 – DO – T2 – Natural Volatiles & Essential Oils JF – Journal JO – JOR SP – 1 EP – 15 VL – 2 IS – 2 SN – -2148-9637 M3 – UR – Y2 – 2019 ER –
EndNote %0 Natural Volatiles & Essential Oils Advanced preparative techniques for the collection of pure components from essential oils %A Danilo Sciarrone , Sebastiano Pantò , Francesco Cacciola , Rosaria Costa , Paola Dugo , Luigi Mondello %T Advanced preparative techniques for the collection of pure components from essential oils %D 2015 %J Natural Volatiles & Essential Oils %P -2148-9637 %V 2 %N 2 %R %U
ISNAD Sciarrone, Danilo , Pantò, Sebastiano , Cacciola, Francesco , Costa, Rosaria , Dugo, Paola , Mondello, Luigi . “Advanced preparative techniques for the collection of pure components from essential oils”. Natural Volatiles & Essential Oils 2 / 2 (June 2015): 1-15.

FULL TEXT: NVEO 2015, Volume 2, Issue 2, Pages 1-15

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